SYNTHESIS METHOD OF PALLADIUM DIBENZYLIDENE ACETONE

The present invention relates to a method for synthesizing palladium dibenzylideneacetone (dba) which comprises the following steps: (a) adding palladium chloride (PdCl_2) and sodium acetate (NaOAc) to a first solvent, and conducts reaction of the two elements to synthesize palladium acetate (Pd (OA...

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Bibliographische Detailangaben
Hauptverfasser: CHANG, JEE YOUNG, YANG, SEUNG HO, YOON, WON KYU, LIM, JAE HOON
Format: Patent
Sprache:eng ; kor
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Zusammenfassung:The present invention relates to a method for synthesizing palladium dibenzylideneacetone (dba) which comprises the following steps: (a) adding palladium chloride (PdCl_2) and sodium acetate (NaOAc) to a first solvent, and conducts reaction of the two elements to synthesize palladium acetate (Pd (OAc)_2); and (b) adding the palladium acetate (Pd (OAc)_2) and the dibenzylideneacetone (dba) to a second solvent, and conducts reaction of the two elements by emitting ultrasonic waves. 본 발명은 팔라듐 디벤질리덴 아세톤의 합성방법에 관한 것으로, 상기 합성방법은, (a) 팔라듐 클로라이드(PdCl)와 나트륨 아세테이트(NaOAc)를 제1 용매에 투입하고, 반응시켜 팔라듐 아세테이트(Pd(OAc))를 합성하는 단계; 및 (b) 상기 팔라듐 아세테이트(Pd(OAc))와 디벤질리덴 아세톤(dba)를 제2 용매에 투입하고, 초음파를 조사하여 반응시키는 단계를 포함한다.