PREPARATION OF DECAHALODIPHENYL ETHANE

This invention provides a process of preparing reaction-derived decahalodiphenylethane of high purity. The process comprises cofeeding separate feeds of (a) diphenylethane and (b) bromine chloride, bromine chloride and bromine, or bromine chloride and chlorine to a refluxing reaction mixture compris...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: HARKINS ALVIN E. JR, BOONE JAMES E
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:This invention provides a process of preparing reaction-derived decahalodiphenylethane of high purity. The process comprises cofeeding separate feeds of (a) diphenylethane and (b) bromine chloride, bromine chloride and bromine, or bromine chloride and chlorine to a refluxing reaction mixture comprising bromine and at least one Lewis acid bromination catalyst so that high purity decahalodiphenylethane is formed.