PREPARATION OF XYLYLENEDIAMINE USING IMIDAZOLE AS A SOLVENT

The present invention relates to a preparation method of xylylenediamine using imidazoles as a solvent, more particularly to a preparation of xylylenediamine by the hydrogenation of phthalonitrile under ammonia atmosphere, wherein an imidazole, which is chemically stable and highly soluble in phthal...

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Bibliographische Detailangaben
Hauptverfasser: LEE, SANG DEUK, CHAE, TAE YOUNG, KIM, HOON SIK, ROW, SUNG WOOK, YOO, KYE SANG, LEE, JE SEUNG
Format: Patent
Sprache:eng
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Zusammenfassung:The present invention relates to a preparation method of xylylenediamine using imidazoles as a solvent, more particularly to a preparation of xylylenediamine by the hydrogenation of phthalonitrile under ammonia atmosphere, wherein an imidazole, which is chemically stable and highly soluble in phthalonitrile, is used as a reaction solvent to significantly reduce the amount of ammonia and obtain high-purity xylylenediamine under mild reaction conditions with high yield.