PRODUCTION OF PRECURSOR PITCH FOR CARBON FIBER
PURPOSE:To obtain the titled pitch of low viscosity with good thermal stability and spinnability without hydrogenation-treatment, etc., by removing the high- molecular weight component in tar pitch by solvent extraction followed by heat-treatment of the resultant pitch. CONSTITUTION:First, tar pitch...
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Zusammenfassung: | PURPOSE:To obtain the titled pitch of low viscosity with good thermal stability and spinnability without hydrogenation-treatment, etc., by removing the high- molecular weight component in tar pitch by solvent extraction followed by heat-treatment of the resultant pitch. CONSTITUTION:First, tar pitch is subjected to extraction-treatment with an aromatic solvent (e.g., tar-based middle oil) followed by separation-treatment such as filtration to eliminate solvent-insolubles. Next, the resulting pitch is treated by heating (pref. being heated to 470-530 deg.C under an inert gas atmo sphere and a reduced pressure =15 deg.C/min. followed by heating at this highest temperature for |
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