MANUFACTURE OF GUAIACOL GLYCERINE ETHER

MANUFACTURE OF GUAIACOL GLYCERINE ETHER

Guaiacol glycerine ether is obtained in very good yield and in very high purity by reacting glycidol with o-methyoxyphenol in the presence of an alkali hydroxide, an alkali alcoholate, an alkali cyanate or an alkali thiocyanate at 80 DEG to 150 DEG C. An especially effective purification of the crud...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: RUDORUFU EMU BUAAGUNAA, ROBAATO ESU NAIGUREN, PEETAA BUERURE, BUORUFUGANGU MERUKU
Format: Patent
Sprache:eng
Schlagworte:
ACYCLIC OR CARBOCYCLIC COMPOUNDS
APPARATUS THEREFOR
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
GENERAL METHODS OF ORGANIC CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
THEIR RELEVANT APPARATUS
TRANSPORTING
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Beschreibung
Zusammenfassung:Guaiacol glycerine ether is obtained in very good yield and in very high purity by reacting glycidol with o-methyoxyphenol in the presence of an alkali hydroxide, an alkali alcoholate, an alkali cyanate or an alkali thiocyanate at 80 DEG to 150 DEG C. An especially effective purification of the crude product can be obtained by adding hydrogen peroxide, preferably prior to cooling.