PRODUCTION OF ORGANIC INDIUM COMPOUND

PRODUCTION OF ORGANIC INDIUM COMPOUND

PROBLEM TO BE SOLVED: To provide a method for producing a crystalline organic indium compound, such as trimethyl indium, in an easy, safe and efficient way. SOLUTION: This method comprises reacting an indium halide with an organic magnesium halogenide in ether solvent to produce an organic indium co...

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Hauptverfasser: OSHIMA MITSUYOSHI, OSAKI HIROMI
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ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
APPARATUS THEREFOR
CHEMISTRY
GENERAL METHODS OF ORGANIC CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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creator OSHIMA MITSUYOSHI
OSAKI HIROMI
description PROBLEM TO BE SOLVED: To provide a method for producing a crystalline organic indium compound, such as trimethyl indium, in an easy, safe and efficient way. SOLUTION: This method comprises reacting an indium halide with an organic magnesium halogenide in ether solvent to produce an organic indium compound expressed by the formula, wherein, a hydrocarbon solvent having a boiling point equal to or less than that of the reaction product, organic indium, then, an indium halide are added to and reacted with ether suspension of an organic magnesium halogenide. In the formula, R is selected from a lower alkyl, phenyl, an alkylsubstituted phenyl, a cyclopentadienyl or an alkyl- substituted cyclopentadienyl. The three R may be the same or different from one another. M represents indium.
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SOLUTION: This method comprises reacting an indium halide with an organic magnesium halogenide in ether solvent to produce an organic indium compound expressed by the formula, wherein, a hydrocarbon solvent having a boiling point equal to or less than that of the reaction product, organic indium, then, an indium halide are added to and reacted with ether suspension of an organic magnesium halogenide. In the formula, R is selected from a lower alkyl, phenyl, an alkylsubstituted phenyl, a cyclopentadienyl or an alkyl- substituted cyclopentadienyl. The three R may be the same or different from one another. 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subjects ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
APPARATUS THEREFOR
CHEMISTRY
GENERAL METHODS OF ORGANIC CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title PRODUCTION OF ORGANIC INDIUM COMPOUND
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