PRODUCTION OF POLYBENZAZOLE FIBER AND POLYBANZAZOLE INTERMEDIATELY DRIED FIBER

PROBLEM TO BE SOLVED: To enable high-speed drying of polybenzazole filaments without damaging to the filaments by coagulating the filaments spun from the dope, washing them with water and drying them under specific conditions. SOLUTION: The spinning dope of a polybenzazole mainly constituted with st...

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Bibliographische Detailangaben
Hauptverfasser: TERAMOTO YOSHIHIKO, KITAGAWA SUSUMU, ISHITOBI MICHIO
Format: Patent
Sprache:eng
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Zusammenfassung:PROBLEM TO BE SOLVED: To enable high-speed drying of polybenzazole filaments without damaging to the filaments by coagulating the filaments spun from the dope, washing them with water and drying them under specific conditions. SOLUTION: The spinning dope of a polybenzazole mainly constituted with structural units of formula I to formula III in a solvent (preferably polyphosphoric acid) is extruded from a spinneret and coagulated through the air gap in the coagulation bath into filaments, which are then washed with water. On the drying, more than 80% of the heating zone is kept at >=240 deg.C and the filaments are dried to some