JPH05310646

PURPOSE:To obtain di-tert-butyl dicarbonate which is useful as a protecting agent for amino groups in high yield from inexpensive starting substances. CONSTITUTION:The process for producing di-tert-butyl dicarbonate is characterized by reaction between an alkali metal mono-tert-butyl carbonate and s...

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Bibliographische Detailangaben
Hauptverfasser: TAKEUCHI HIROSHI, MASUMI FUMIO, HIGASHIYAMA KAZUYUKI, HARUYAMA SATORU
Format: Patent
Sprache:eng
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Zusammenfassung:PURPOSE:To obtain di-tert-butyl dicarbonate which is useful as a protecting agent for amino groups in high yield from inexpensive starting substances. CONSTITUTION:The process for producing di-tert-butyl dicarbonate is characterized by reaction between an alkali metal mono-tert-butyl carbonate and sulfonyl chloride in the presence of an aprotic polar solvent and a base.