JPH05310646
PURPOSE:To obtain di-tert-butyl dicarbonate which is useful as a protecting agent for amino groups in high yield from inexpensive starting substances. CONSTITUTION:The process for producing di-tert-butyl dicarbonate is characterized by reaction between an alkali metal mono-tert-butyl carbonate and s...
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Sprache: | eng |
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Zusammenfassung: | PURPOSE:To obtain di-tert-butyl dicarbonate which is useful as a protecting agent for amino groups in high yield from inexpensive starting substances. CONSTITUTION:The process for producing di-tert-butyl dicarbonate is characterized by reaction between an alkali metal mono-tert-butyl carbonate and sulfonyl chloride in the presence of an aprotic polar solvent and a base. |
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