JPH0372568B
PURPOSE:To prepare uniform, porous, and spherical carbon, by granulating a petroleum aromatic resin substance obtained from a proper petroleum fraction, extracting and removing a low-molecular-weight component from it to give a porous resin substance, making the substance infusible, calcining it in...
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Zusammenfassung: | PURPOSE:To prepare uniform, porous, and spherical carbon, by granulating a petroleum aromatic resin substance obtained from a proper petroleum fraction, extracting and removing a low-molecular-weight component from it to give a porous resin substance, making the substance infusible, calcining it in an inert atmosphere. CONSTITUTION:A fraction rich in aromatic components obtained by extraction from a petroleum fraction having 150-850 average molecular weight with furfural, phenol, or methylpyrrolidone is brought into contact with oxygen or an oxygen-containing gas or a gas containing oxygen and ozone at 200-380 deg.C, it is dehydrogenated, and subjected to polycondensation, to give a petroleum aromatic resin substance having 80-220 deg.C softening point. This resin substance is granulated by granulation of heating, melting and dispersion, a low-molecular-weight component in it is extracted with a solvent such as methanol, etc. at normal temperature to give a high-softening, uniform, porous resin substance, which is made infusible by the use of an oxidizing agent such as air, etc. at normal temperature - at 400 deg.C, and calcined at |
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