PULVERIZATION OF POLY-BETA-ALANINE COPOLYMER

PURPOSE:To easily obtain the subject uniform copolymer having small average particle diameter and narrow particle size distribution at a low cost by carrying coarse particles of poly-beta-alanine copolymer on a jet stream and subjecting the particles to collision and pulverization. CONSTITUTION:Coar...

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Bibliographische Detailangaben
Hauptverfasser: HANEZAWA HIROSHI, OTAKE JUNZO
Format: Patent
Sprache:eng
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Zusammenfassung:PURPOSE:To easily obtain the subject uniform copolymer having small average particle diameter and narrow particle size distribution at a low cost by carrying coarse particles of poly-beta-alanine copolymer on a jet stream and subjecting the particles to collision and pulverization. CONSTITUTION:Coarse particles of a poly-beta-alanine copolymer having a reduced viscosity (etaSP/C) of 0.2-15dl/g are pulverized in a jet mill pulverizer, etc., using a dehumidified air, inert gas, etc., having a water content of 1,000 to 500ppm or less at a jet stream velocity of Mach 0.5 to 5.0 (preferably Mach 1 to 3) and classified with a classifier to obtain the objective copolymer having an average particle diameter of 1.0 to 10.0mum. The pulverization and classification are repeated until the particle size reaches the target level.