MANUFACTURING METHOD OF HETEROPOLY-ACID BASED CATALYST FOR MANUFACTURING METHACRYLIC ACID
PROBLEM TO BE SOLVED: To easily and inexpensively manufacture a heteropoly-acid based catalyst for manufacturing methacrylic acid from the used heteropoly-acid based catalyst for manufacturing methacrylic acid at a yield of 90% ore higher relative to an unused one. SOLUTION: The manufacturing method...
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Zusammenfassung: | PROBLEM TO BE SOLVED: To easily and inexpensively manufacture a heteropoly-acid based catalyst for manufacturing methacrylic acid from the used heteropoly-acid based catalyst for manufacturing methacrylic acid at a yield of 90% ore higher relative to an unused one. SOLUTION: The manufacturing method of the heteropoly-acid based catalyst for manufacturing methacrylic acid has a separation step for contacting the used heteropoly-acid based catalyst containing one kind or more of elements selected from the group consisting of cesium, potassium, thallium and rubidium and molybdenum and used for manufacturing of methacrylic acid by vapor phase contact oxidation with an aqueous medium of pH 1 to less than pH 8, and solid/liquid-separating the obtained dispersion to a liquid component and a solid recovery component, and a catalyst preparation step for preparing the heteropoly-acid based catalyst for manufacturing methacrylic acid making the solid recovery component as a material. COPYRIGHT: (C)2008,JPO&INPIT |
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