METHOD FOR PRODUCING DIANHYDROHEXITOL-BIS-(4- ACRYLOYLOXY)ACYLATE

METHOD FOR PRODUCING DIANHYDROHEXITOL-BIS-(4- ACRYLOYLOXY)ACYLATE

PROBLEM TO BE SOLVED: To provide a method for producing dianhydrohexitol-bis-(4-acryloyloxy) acylate represented by general formula 2. SOLUTION: In a first process, dianhydrohexitol bisacylate represented by general formula 3 is biacylated using a 3-halopropionyl halide, yielding the corresponding d...

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Bibliographische Detailangaben
Hauptverfasser: KRIEGBAUM MARKUS, BRADER LEONHARD, HAEBERLE NORMAN
Format: Patent
Sprache:eng
Schlagworte:
CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
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Zusammenfassung:PROBLEM TO BE SOLVED: To provide a method for producing dianhydrohexitol-bis-(4-acryloyloxy) acylate represented by general formula 2. SOLUTION: In a first process, dianhydrohexitol bisacylate represented by general formula 3 is biacylated using a 3-halopropionyl halide, yielding the corresponding dianhydrohexitol-bis-[3-halopropionyloxy]arylate and in a second process, two hydrogen halide molecules are cleaved from the dianhydrohexitol- bis-[3-halopropionyloxy]arylate with the aid of a base. Consequently, high-purity dianhydrohexitol-bis-(4-acryloyloxy)acylate represented by general formula 2 is inexpensively obtained by an industrially simple method in a high yield.