METHOD FOR REFINING SPONGE TITANIUM AND DEVICE THEREFOR
PROBLEM TO BE SOLVED: To provide a refining method by which, at the time of separating impurities such as magnesium chloride and metallic magnesium remaining in a sponge titanium at high temperature under the reduced pressure, introducing the impurities into a capacitor vessel and performing condens...
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Sprache: | eng |
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Zusammenfassung: | PROBLEM TO BE SOLVED: To provide a refining method by which, at the time of separating impurities such as magnesium chloride and metallic magnesium remaining in a sponge titanium at high temperature under the reduced pressure, introducing the impurities into a capacitor vessel and performing condensation, thereby separating the same away, a separating vessel is not deformed, and to provide a vacuum separating device. SOLUTION: In this refining method in which, as for the sponge titanium obtained by bringing metallic magnesium into reaction with titanium tetrachloride in a separating vessel 5 contained in a heating furnace, impuritis are removed under a reduced pressure, the pressure in the heating furnace 1 and the separating vessel 5 is reduced, and furthere, in the process of the pressure reduction, the pressure in the separating vessel 5 is made the same as that in a space part 1a between the separating vessel 5 and the heating furnace 1 or higher than that. |
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