METHOD FOR MANUFACTURING CATALYST FOR SYNTHESIZING FORMALDEHYDE SYNTHESIS
PROBLEM TO BE SOLVED: To provide a method for manufacturing a ferrimolybdate catalyst for synthesis of formaldehyde by oxidizing methanol by an excess air method at a high conversion rate and a high selectivity and prolonging its service life. SOLUTION: An aqueous solution of iron (III) salt is adde...
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Zusammenfassung: | PROBLEM TO BE SOLVED: To provide a method for manufacturing a ferrimolybdate catalyst for synthesis of formaldehyde by oxidizing methanol by an excess air method at a high conversion rate and a high selectivity and prolonging its service life. SOLUTION: An aqueous solution of iron (III) salt is added to an aqueous solution of a molybate to produce a slurry solution of a Mo/Fe molar ratio of 1.4-1.6. The slurry solution is subjected to a hydrothermal reaction at a temperature of 70 deg.C-boiling point for 2-10 h. Produced ferrimolybdate crystal is filtered, washed and dried, and it is molded, or carried on a carrier, and burned at 500-650 deg.C for 2-6 h to obtain an oxidation catalyst. |
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