PRODUCTION OF ALKYLPHOSPHONOUS ACID (METAL) SALT

PROBLEM TO BE SOLVED: To provide a method for producing an alkylphosphonous acid (metal) salt easily, uniformly and in high yield. SOLUTION: This method comprises reacting elemental yellow phosphorus with a halogen-free alkylating agent in the presence of at least one base; wherein it is preferable...

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Hauptverfasser: WEFERLING NORBERT DR, SICKEN MARTIN
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creator WEFERLING NORBERT DR
SICKEN MARTIN
description PROBLEM TO BE SOLVED: To provide a method for producing an alkylphosphonous acid (metal) salt easily, uniformly and in high yield. SOLUTION: This method comprises reacting elemental yellow phosphorus with a halogen-free alkylating agent in the presence of at least one base; wherein it is preferable that the reaction is carried out in a two-phase system comprising the above base(s) and an organic solvent, and the alkylating agent is a dialkyl sulfate, trialkyl phosphate, dialkyl carbonate and/or formic orthoester.
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subjects ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAININGELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN,SULFUR, SELENIUM OR TELLURIUM
ADHESIVES
APPARATUS THEREFOR
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
COMPOSITIONS BASED THEREON
COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
DYES
GENERAL METHODS OF ORGANIC CHEMISTRY
MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FORELSEWHERE
METALLURGY
MISCELLANEOUS APPLICATIONS OF MATERIALS
MISCELLANEOUS COMPOSITIONS
NATURAL RESINS
ORGANIC CHEMISTRY
ORGANIC MACROMOLECULAR COMPOUNDS
PAINTS
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
POLISHES
THEIR PREPARATION OR CHEMICAL WORKING-UP
THEIR RELEVANT APPARATUS
TRANSPORTING
USE OF INORGANIC OR NON-MACROMOLECULAR ORGANIC SUBSTANCES ASCOMPOUNDING INGREDIENTS
title PRODUCTION OF ALKYLPHOSPHONOUS ACID (METAL) SALT
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