PRODUCTION OF ETHYLENE GLYCOL SOLUBLE GERMANIUM DIOXIDE AND DISSOLVING METHOD THEREOF

PROBLEM TO BE SOLVED: To produce a crystalline germanium dioxide having excellent solubility in the producing method of a catalyst solution for polyester production in high yield by hydrolyzing germanium tetrachloride under a specific condition. SOLUTION: In the reaction for producing the crystallin...

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Hauptverfasser: ORI AIICHIRO, KAYA MASARU
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KAYA MASARU
description PROBLEM TO BE SOLVED: To produce a crystalline germanium dioxide having excellent solubility in the producing method of a catalyst solution for polyester production in high yield by hydrolyzing germanium tetrachloride under a specific condition. SOLUTION: In the reaction for producing the crystalline germanium dioxide by hydrolyzing germanium tetrachloride, germanium tetrachloride and water are mixed with each other at 0-20 deg.C, and then, the reaction mixture is kept at 0-20 deg.C for 1-48 hr. The germanium catalyst solution for polyester production is produced by removing produced water from the reaction liquid in the reaction to dissolve the produced crystalline germanium dioxide into ethylene glycol.
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SOLUTION: In the reaction for producing the crystalline germanium dioxide by hydrolyzing germanium tetrachloride, germanium tetrachloride and water are mixed with each other at 0-20 deg.C, and then, the reaction mixture is kept at 0-20 deg.C for 1-48 hr. 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subjects CHEMISTRY
COMPOSITIONS BASED THEREON
COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSESC01D OR C01F
INORGANIC CHEMISTRY
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
METALLURGY
ORGANIC MACROMOLECULAR COMPOUNDS
THEIR PREPARATION OR CHEMICAL WORKING-UP
title PRODUCTION OF ETHYLENE GLYCOL SOLUBLE GERMANIUM DIOXIDE AND DISSOLVING METHOD THEREOF
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