DETECTING METHOD OF POLYBIPHENYL CHLORIDE

PROBLEM TO BE SOLVED: To perform a detection with sufficient precision by setting the temperature of a separation tube to a specified range when a sample containing polybiphenyl chloride (PCB) is passed in the separation tube. SOLUTION: This methods comprises a carrier gas supplying means 1, a detec...

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Bibliographische Detailangaben
Hauptverfasser:	SHIMURA MITSUHIKO, NAKAJIMA TOSHIO, TOMA TOSHIYOSHI
Format:	Patent
Sprache:	eng
Schlagworte:	CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES MEASURING PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL PHYSICS TESTING THEIR RELEVANT APPARATUS TRANSPORTING
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Beschreibung
Zusammenfassung:	PROBLEM TO BE SOLVED: To perform a detection with sufficient precision by setting the temperature of a separation tube to a specified range when a sample containing polybiphenyl chloride (PCB) is passed in the separation tube. SOLUTION: This methods comprises a carrier gas supplying means 1, a detecting means (radiation source) 3 connected to the carrier gas supplying means 1, a separation tube (column) 4 having one end side connected to the carrier gas supplying means 1 through the detecting means 3, and a recorder 5 connected to the detecting means 3. Further, it comprises a sample injecting means 6, so that the sample injection means 6 supplies a sample containing PCB or a treated insulating oil to a sample injection port 7 provided on one end of the separation tube 4. A flowmeter 8 is connected to the other end of the separation tube 4 through the detecting means. When the sample containing PCG is passed through the separation tube 4 of a gas chromatographic device, the temperature of the separation tube 4 is set to 170-190 deg.C, particularly to 175-185 deg.C.