PRODUCTION OF CYCLIC ALCOHOL

PROBLEM TO BE SOLVED: To produce a cyclic alcohol at a high reactional rate and a resultantly improved rate of reaction. SOLUTION: A cycloalkane having 9-16 carbon atoms and boric acid in an amount of 0.2-5 mass % based on the cycloalkane are charged and the boric acid in an amount so as to provide...

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Bibliographische Detailangaben
Hauptverfasser:	GUENZEL BERND DR, GRUND GERDA
Format:	Patent
Sprache:	eng
Schlagworte:	ACYCLIC OR CARBOCYCLIC COMPOUNDS APPARATUS THEREFOR CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY CHEMISTRY GENERAL METHODS OF ORGANIC CHEMISTRY METALLURGY ORGANIC CHEMISTRY PERFORMING OPERATIONS PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL THEIR RELEVANT APPARATUS TRANSPORTING
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Beschreibung
Zusammenfassung:	PROBLEM TO BE SOLVED: To produce a cyclic alcohol at a high reactional rate and a resultantly improved rate of reaction. SOLUTION: A cycloalkane having 9-16 carbon atoms and boric acid in an amount of 0.2-5 mass % based on the cycloalkane are charged and the boric acid in an amount so as to provide (1:0.6) to (1:1.7) molar ratio of the formed cyclic alcohol to the boric acid at the completion of the reaction are metered and fed during the reaction in a method for oxidizing the cycloalkane into the cyclic alcohol in the presence of the boric acid using an oxygen-containing gas. Furthermore, the reaction is conducted in the presence of 0.05-5 mass % of cobalt (II) based on the essentially used cycloalkane.