4-Amino-2,2,6,6-tetra:methyl piperidine prepn
4-Amino-2,2,6,6-tetramethyl piperidine (I) is prepd. by reacting 2,2,6,6-tetramethyl -4-oxopiperidine (II) with NH3 and H2 at 100-135 deg.C and a pressure of 10-25 bar in an aq. medium in the presence of a hydrogenation catalyst (III) and 1-2 wt.% (w.r.t. (III)) of an alkali(ne earth) metal hydroxid...
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Zusammenfassung: | 4-Amino-2,2,6,6-tetramethyl piperidine (I) is prepd. by reacting 2,2,6,6-tetramethyl -4-oxopiperidine (II) with NH3 and H2 at 100-135 deg.C and a pressure of 10-25 bar in an aq. medium in the presence of a hydrogenation catalyst (III) and 1-2 wt.% (w.r.t. (III)) of an alkali(ne earth) metal hydroxide. |
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