PROCESS FOR PURIFYING 5H-DIBENZO-(B,F)-AZEPINE

PROCESS FOR PURIFYING 5H-DIBENZO-(B,F)-AZEPINE

Purificn. of iminostilbene (I) comprises: (a) evapn. of (I) from a reaction mixt. obtd. by catalytic dehydrogenation of iminodibenzyl (II) and sepn. of solid prod. obtd.; (b) suspension of the solid prod. in an aromatic hydrocarbon; and (c) isolation of pure (I).

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Bibliographische Detailangaben
Hauptverfasser: EICHBERGER,GUENTHER, RAML,WALTER
Format: Patent
Sprache:eng
Schlagworte:
CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
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Beschreibung
Zusammenfassung:Purificn. of iminostilbene (I) comprises: (a) evapn. of (I) from a reaction mixt. obtd. by catalytic dehydrogenation of iminodibenzyl (II) and sepn. of solid prod. obtd.; (b) suspension of the solid prod. in an aromatic hydrocarbon; and (c) isolation of pure (I).