PROCESS FOR PRODUCTION OF 1-BENZIL-CYCLOHEPTHAN-1-OL

PROCESS FOR PRODUCTION OF 1-BENZIL-CYCLOHEPTHAN-1-OL

1-benzyl-cycloheptan-1-ol is prepd. by the Grignard reaction of benzylchloride and cycloheptanone and the decompsn. of the Grignard cpd., by adding the mixt. of benzyl-chloride and cycloheptanone opt. diluted with an aromatic hydrocarbon at 60-100 deg.C to a mixt. of magnesium metal, an ether boilin...

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Bibliographische Detailangaben
Hauptverfasser: BALAZS,TIVADAR,HU, TOEROEK,MIKLOS,HU, ZAGON,TAMAS,HU, TOEMPE,JANOS,HU, VARGA,MIKLOS,HU, DROZDIK,GYOERGY,HU, FERTOEDI,BELANE,HU, BUDAI,ZOLTANNE,HU
Format: Patent
Sprache:eng
Schlagworte:
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
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Zusammenfassung:1-benzyl-cycloheptan-1-ol is prepd. by the Grignard reaction of benzylchloride and cycloheptanone and the decompsn. of the Grignard cpd., by adding the mixt. of benzyl-chloride and cycloheptanone opt. diluted with an aromatic hydrocarbon at 60-100 deg.C to a mixt. of magnesium metal, an ether boiling above 45 deg. C and an aromatic hydrocarbon, and decomposing the Grignard cpd. formed in situ in the known way.