PROCESS FOR THE PURIFICATION OF ACRYLIC ACID

PROCESS FOR THE PURIFICATION OF ACRYLIC ACID

A process and an apparatus for the purification of a crude acrylic acid composition containing maleic anhydride as an impurity comprising the following steps: (a) carrying out at least one dynamic melt crystallization stage (14, 14a, 14b, 14c, 14d) with the crude acrylic acid composition to prepare...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: KUSZLIK, Andrzej, ENGSTLER, Herbert, LIPPUNER, Florian, SCHÄFER, Matthias
Format: Patent
Sprache:eng ; hun
Schlagworte:
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
SEPARATION
TRANSPORTING
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Beschreibung
Zusammenfassung:A process and an apparatus for the purification of a crude acrylic acid composition containing maleic anhydride as an impurity comprising the following steps: (a) carrying out at least one dynamic melt crystallization stage (14, 14a, 14b, 14c, 14d) with the crude acrylic acid composition to prepare a first purified acrylic acid composition and a first residue containing at least 3.5 % by weight maleic anhydride, (b) adding a solvent (26) to the first residue in an amount that the weight ratio of the solvent to the maleic anhydride is 0.3 or more to prepare a ratio-adjusted residue and (c) carrying out at least one further dynamic melt crystallization stage and/ or at least one static melt crystallization stage (18, 18a, 18b) with the ratio-adjusted residue to prepare a second purified acrylic acid composition and a second residue.