PROCEDE D'OBTENTION DE PRECURSEURS DE CERAMIQUES SUPRACONDUCTRICES A HAUTE TEMPERATURE CRITIQUE
Process for obtaining precursors for high critical temperature superconductor ceramics, by precipitation of water-insoluble salts, characterised in that it comprises the following stages: - the starting point is a solution of soluble salts where the cations are found in stoichiometric proportions...
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Zusammenfassung: | Process for obtaining precursors for high critical temperature superconductor ceramics, by precipitation of water-insoluble salts, characterised in that it comprises the following stages:
- the starting point is a solution of soluble salts where the cations are found in stoichiometric proportions of the desired superconductor phase,
- a first complete precipitation is carried out of a first series of cations at a first pH value,
- the first precipitate obtained is filtered, washed and the filtrate retained,
- a second value is given to the pH of the said filtrate and the residual cations are precipitated,
- the second precipitate is filtered,
- the first and second precipitates are homogenised,
- the product obtained is dried, calcined and crushed. |
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