COMPOSITIONS INCLUDING COPOLYMERS OF ISOBUTYLENE AND PARAMETHYLSTYRENE SUBSTANTIALLY FREE OF PARAMETHYLSTYRENE MONOMERS AND METHODS OF MAKING THE SAME
A process for preparing a cement composition comprising an isoolefin-alkylstyrene copolymer and substantially free of an alkylstyrene monomer is described herein. The process comprises reacting the isoolefin monomer with at least a portion of the alkylstyrene monomer in a diluent to form an isoolefi...
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Format: | Patent |
Sprache: | eng ; fre ; ger |
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Zusammenfassung: | A process for preparing a cement composition comprising an isoolefin-alkylstyrene copolymer and substantially free of an alkylstyrene monomer is described herein. The process comprises reacting the isoolefin monomer with at least a portion of the alkylstyrene monomer in a diluent to form an isoolefin-alkylstyrene copolymer, replacing the diluent with a solvent, reacting a halogenic scavenger with the unreacted alkylstyrene monomer in an absence of a free radical initiator in order to form a halogenic alkylstyrene compound without altering the isoolefin- alkylstyrene copolymer, and removing the halogenic alkylstyrene compound from the slurry to form the cement composition substantially free of the alkylstyrene monomer. Also disclosed herein is a composition comprising an isoolefin-alkylstyrene copolymer and an alkylstyrene monomer comprising a concentration less than about 20 ppm. |
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