METHOD FOR RECOVERING LITHIUM FROM LITHIUM PRECIPITATION MOTHER LIQUOR

A method for recovering lithium from a mother liquor after lithium carbonate precipitation reaction, the method using the following cycle steps including adsorption, displacement, desorption and transformation: a. adding a lithium-sodium separation resin into resin columns, and feeding the mother li...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: YAN, Hudao, LI, Suidang, FAN, Lili, WEI, Yuyun, LYU, Weiqiang, YU, Jia, LIU, Qiong, GUO, Fumin, GAO, Junlin, KOU, Xiaokang
Format: Patent
Sprache:eng ; fre ; ger
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:A method for recovering lithium from a mother liquor after lithium carbonate precipitation reaction, the method using the following cycle steps including adsorption, displacement, desorption and transformation: a. adding a lithium-sodium separation resin into resin columns, and feeding the mother liquor after lithium carbonate precipitation reaction to the resin columns for adsorption, wherein the adsorption rate can reach 90% or more; b. after adsorption, washing the resin with water, displacing the sodium ion with a lithium ion by lithium solution to wash out residual sodium from the resin; c. after displacement, desorbing the resin by means of an acid solution to obtain a qualified desorption solution with a high lithium and low sodium content; and d. after desorption, carrying out reverse transformation in the resin by means of a transformation solution in order to ensure that no bubbles appear and then maintain the adsorption effect during the adsorption process. During the cycle, the lithium in the mother liquor after lithium carbonate precipitation reaction was separated from the solution with a high sodium-to-lithium ratio to obtain the solution with the high lithium-to-sodium ratio.