PROCESS FOR PRODUCING MONOCHLOROACETIC ACID FROM GLYCOLIC ACID

The disclosure is directed to a process for producing monochloroacetic acid from glycolic acid comprising contacting a liquid medium comprising glycolic acid and water with a hydrogen chloride-containing gas stream, resulting in the formation of a liquid medium into which hydrogen chloride has been...

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Hauptverfasser: PATIL, Bhaskar Sudhakar, RENKEMA, Eilertdina Henderika, VENEMAN, Rens, TEN KATE, Antoon Jacob Berend, VAN LARE, Cornelis Elizabeth Johannus, DIRIX, Carolina Anna Maria Christina, AHR, Mathieu Pierre
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creator PATIL, Bhaskar Sudhakar
RENKEMA, Eilertdina Henderika
VENEMAN, Rens
TEN KATE, Antoon Jacob Berend
VAN LARE, Cornelis Elizabeth Johannus
DIRIX, Carolina Anna Maria Christina
AHR, Mathieu Pierre
description The disclosure is directed to a process for producing monochloroacetic acid from glycolic acid comprising contacting a liquid medium comprising glycolic acid and water with a hydrogen chloride-containing gas stream, resulting in the formation of a liquid medium into which hydrogen chloride has been absorbed, and reacting the glycolic acid with the absorbed hydrogen chloride at a temperature of from about 120 °C to about 180 °C and at an absolute pressure of from about 0.5 MPa to about 2 MPa, wherein the hydrogen chloride-containing gas stream is provided during at least part of the absorption step and at least part of the reaction step in a continuous manner or intermittently in at least 2 portions.
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subjects ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
title PROCESS FOR PRODUCING MONOCHLOROACETIC ACID FROM GLYCOLIC ACID
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