METHODS FOR PRODUCING LACTIDE WITH RECRYSTALLIZATION AND RECYCLE OF MESO-LACTIDE

Polylactides are formed by forming and depolymerizing a low molecular weight poly(lactic acid) to form a crude lactide, separating meso-lactide to form a meso-lactide stream that is enriched in impurities, purifying the meso-lactide-enriched stream by melt crystallization, recombining at least a por...

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Bibliographische Detailangaben
Hauptverfasser: BENSON, Richard Douglas, SCHROEDER, Joseph D
Format: Patent
Sprache:eng ; fre ; ger
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Zusammenfassung:Polylactides are formed by forming and depolymerizing a low molecular weight poly(lactic acid) to form a crude lactide, separating meso-lactide to form a meso-lactide stream that is enriched in impurities, purifying the meso-lactide-enriched stream by melt crystallization, recombining at least a portion of the purified meso-lactide stream with an S,S- and R,R-lactide stream and polymerizing the recombined streams.