PROCESS AND CONTIUOUS FLOW SYSTEM FOR PREARING SODIUM 5-NITROTETRAZOLE AT A RATE OF AT LEAST 100 GRAM/HOUR AND AT A TEMPERATURE OF 10-30 °C

PROCESS AND CONTIUOUS FLOW SYSTEM FOR PREARING SODIUM 5-NITROTETRAZOLE AT A RATE OF AT LEAST 100 GRAM/HOUR AND AT A TEMPERATURE OF 10-30 °C

Described are methods for preparing salts of 5-nitrotetrazolate that include reacting aqueous solutions of 5-aminotetrazole, an acid, and sodium nitrite in a continuous flow system at an ambient temperature.

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Bibliographische Detailangaben
Hauptverfasser: BRAGG, Jon G, FRONABARGER, John W, PATTISON, Jason B, WILLIAMS, Michael D
Format: Patent
Sprache:eng ; fre ; ger
Schlagworte:
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOIDCHEMISTRY
CHEMISTRY
HETEROCYCLIC COMPOUNDS
METALLURGY
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
THEIR RELEVANT APPARATUS
TRANSPORTING
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Beschreibung
Zusammenfassung:Described are methods for preparing salts of 5-nitrotetrazolate that include reacting aqueous solutions of 5-aminotetrazole, an acid, and sodium nitrite in a continuous flow system at an ambient temperature.