METHOD FOR PREPARING D-PSICOSE CRYSTAL

A method for producing high purity D-psicose crystals having a purity of 98% (w/w) or more and a grain size of MA200 or more. The method includes: removing impurities from a D-psicose solution to obtain a purified D-psicose solution; concentrating the purified D-psicose solution; cooling the concent...

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Bibliographische Detailangaben
Hauptverfasser: KIM, Seong Bo, AN, Jun Gap, LEE, Joo Hang, PARK, Seung Won
Format: Patent
Sprache:eng ; fre ; ger
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Beschreibung
Zusammenfassung:A method for producing high purity D-psicose crystals having a purity of 98% (w/w) or more and a grain size of MA200 or more. The method includes: removing impurities from a D-psicose solution to obtain a purified D-psicose solution; concentrating the purified D-psicose solution; cooling the concentrated D-psicose solution to 30°C to 40°C through a heat exchanger; seed crystallizing the D-psicose solution at 30°C to 40°C to obtain a seed crystallized massecuite; and full-scale crystallizing the seed crystallized massecuite. The method can produce pure D-psicose crystals in a suitable form for industrial application through an economical crystallization process from the D-psicose solution without using organic solvents.