RECOVERY OF CARBOXYLIC ACID FROM THEIR MAGNESIUM SALTS BY PRECIPITATION USING HYDROCHLORIC ACID, USEFUL FOR FERMENTATION BROTH WORK-UP

A method for preparing a carboxylic acid, includes the steps of: providing magnesium carboxylate, wherein the carboxylic acid corresponding with the carboxylate is selected from the group made of 2,5-furandicarboxylic acid, fumaric acid, adipic acid, itaconic acid, citric acid, glutaric acid, maleic...

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Hauptverfasser: CERDÀ BARÓ, Agustín, VAN BREUGEL, Jan, VIDAL LANCIS, José María, DE HAAN, André Banier, JANSEN, Peter Paul, VAN DER WEIDE, Paulus Loduvicus Johannes
Format: Patent
Sprache:eng ; fre ; ger
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Zusammenfassung:A method for preparing a carboxylic acid, includes the steps of: providing magnesium carboxylate, wherein the carboxylic acid corresponding with the carboxylate is selected from the group made of 2,5-furandicarboxylic acid, fumaric acid, adipic acid, itaconic acid, citric acid, glutaric acid, maleic acid, malonic acid, oxalic acid and fatty acids having more than 10 carbon atoms; acidifying the magnesium carboxylate with hydrogen chloride (HCl), thereby obtaining a solution including carboxylic acid and magnesium chloride (MgCl2); optionally a concentration step, wherein the solution including carboxylic acid and MgCl2 is concentrated; and precipitating the carboxylic acid from the solution including the carboxylic acid and MgCl2, thereby obtaining a carboxylic acid precipitate and a MgCl2 solution.