Method for activating double metal cyanide catalysts to produce polyether polyols
Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under...
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creator | LEITNER, WALTER DR BARRUET, JULIEN DR MUELLER, THOMAS, ERNST DR GUERTLER, CHRISTOPH DR KOEHLER, BURKHARD DR DIENES, YVONNE DR |
description | Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or a pure carbon dioxide atmosphere, (b) adding alkylene oxide to the mixture obtained in the step (a), and (c) continuously adding at least one alkylene oxide and carbon dioxide to the mixture obtained in the step (b). Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or under a pure carbon dioxide atmosphere, at 90-150[deg] C, (b) adding alkylene oxide to the mixture obtained in the step (a) under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or a pure carbon dioxide atmosphere, at 100-150[deg] C, and (c) continuously adding at least one alkylene oxide and carbon dioxide to the mixture obtained in the step (b). An independent claim is also included for activating DMC catalyst, comprising (i) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under inert gas, atmosphere of inert gas-carbon dioxide mixture, or pure carbon dioxide atmosphere, and subsequently (ii) adding alkylene oxide to the mixture obtained in the step (i) under an inert gas, an atmosphere of inert gas-carbon dioxide mixture, or a pure carbon dioxide atmosphere at 90-150[deg] C.
Die vorliegende Erfindung betrifft ein Verfahren zur Aktivierung von Doppelmetallcyanid (DMC)-Katalysatoren mit Heterokumulenen für die Herstellung von Polyethercarbonatpolyolen durch katalytische Copolymerisation von Kohlendioxid (CO 2 ) mit Alkylenoxiden in Gegenwart einer oder mehrerer H-funktioneller Startersubstanzen, sowie ein Verfahren zur Herstellung von Polyethercarbonatpolyolen aus einer oder mehreren H-funktionellen Startersubstanzen, eines oder mehrerer Alkylenoxiden und Kohlendioxid in Gegenwart eines Doppelmetallcyanid-Katalysators, dadurch gekennzeichnet, dass
(±) unter Inertgasatmosphäre, unter einer Atmosphäre aus Inertgas-Kohlendioxid-Gemisch oder unter einer re |
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fullrecord | <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_EP2548905A1</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>EP2548905A1</sourcerecordid><originalsourceid>FETCH-epo_espacenet_EP2548905A13</originalsourceid><addsrcrecordid>eNrjZAj0TS3JyE9RSMsvUkhMLsksSyzJzEtXSMkvTcpJVchNLUnMUUiuTMzLTElVSE4E8iqLS4oVSvIVCoryU0qTUxUK8nMqgUakFoFZ-TnFPAysaYk5xam8UJqbQcHNNcTZQze1ID8-tbggMTk1L7Uk3jXAyNTEwtLA1NHQmAglAKwaN_o</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>Method for activating double metal cyanide catalysts to produce polyether polyols</title><source>esp@cenet</source><creator>LEITNER, WALTER DR ; BARRUET, JULIEN DR ; MUELLER, THOMAS, ERNST DR ; GUERTLER, CHRISTOPH DR ; KOEHLER, BURKHARD DR ; DIENES, YVONNE DR</creator><creatorcontrib>LEITNER, WALTER DR ; BARRUET, JULIEN DR ; MUELLER, THOMAS, ERNST DR ; GUERTLER, CHRISTOPH DR ; KOEHLER, BURKHARD DR ; DIENES, YVONNE DR</creatorcontrib><description>Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or a pure carbon dioxide atmosphere, (b) adding alkylene oxide to the mixture obtained in the step (a), and (c) continuously adding at least one alkylene oxide and carbon dioxide to the mixture obtained in the step (b). Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or under a pure carbon dioxide atmosphere, at 90-150[deg] C, (b) adding alkylene oxide to the mixture obtained in the step (a) under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or a pure carbon dioxide atmosphere, at 100-150[deg] C, and (c) continuously adding at least one alkylene oxide and carbon dioxide to the mixture obtained in the step (b). An independent claim is also included for activating DMC catalyst, comprising (i) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under inert gas, atmosphere of inert gas-carbon dioxide mixture, or pure carbon dioxide atmosphere, and subsequently (ii) adding alkylene oxide to the mixture obtained in the step (i) under an inert gas, an atmosphere of inert gas-carbon dioxide mixture, or a pure carbon dioxide atmosphere at 90-150[deg] C.
Die vorliegende Erfindung betrifft ein Verfahren zur Aktivierung von Doppelmetallcyanid (DMC)-Katalysatoren mit Heterokumulenen für die Herstellung von Polyethercarbonatpolyolen durch katalytische Copolymerisation von Kohlendioxid (CO 2 ) mit Alkylenoxiden in Gegenwart einer oder mehrerer H-funktioneller Startersubstanzen, sowie ein Verfahren zur Herstellung von Polyethercarbonatpolyolen aus einer oder mehreren H-funktionellen Startersubstanzen, eines oder mehrerer Alkylenoxiden und Kohlendioxid in Gegenwart eines Doppelmetallcyanid-Katalysators, dadurch gekennzeichnet, dass
(±) unter Inertgasatmosphäre, unter einer Atmosphäre aus Inertgas-Kohlendioxid-Gemisch oder unter einer reinen Kohlendioxid-Atmosphäre bei Temperaturen von 90 bis 150°C der DMC-Katalysator mit Heterokumulen und H-funktioneller Startersubstanz vermischt wird,
(²) zu dem Gemisch aus Schritt (±) unter Inertgasatmosphäre, unter einer Atmosphäre aus Inertgas-Kohlendioxid-Gemisch oder unter einer reinen Kohlendioxid-Atmosphäre Alkylenoxid bei Temperaturen von 100 bis 150°C zugegeben wird, und
(³) ein oder mehrere Alkylenoxide und Kohlendioxid zu der aus Schritt (²) resultierenden Mischung fortwährend dosiert werden.</description><language>eng ; fre ; ger</language><subject>CHEMISTRY ; COMPOSITIONS BASED THEREON ; MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS ; METALLURGY ; ORGANIC MACROMOLECULAR COMPOUNDS ; THEIR PREPARATION OR CHEMICAL WORKING-UP</subject><creationdate>2013</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20130123&DB=EPODOC&CC=EP&NR=2548905A1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,780,885,25564,76547</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&date=20130123&DB=EPODOC&CC=EP&NR=2548905A1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>LEITNER, WALTER DR</creatorcontrib><creatorcontrib>BARRUET, JULIEN DR</creatorcontrib><creatorcontrib>MUELLER, THOMAS, ERNST DR</creatorcontrib><creatorcontrib>GUERTLER, CHRISTOPH DR</creatorcontrib><creatorcontrib>KOEHLER, BURKHARD DR</creatorcontrib><creatorcontrib>DIENES, YVONNE DR</creatorcontrib><title>Method for activating double metal cyanide catalysts to produce polyether polyols</title><description>Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or a pure carbon dioxide atmosphere, (b) adding alkylene oxide to the mixture obtained in the step (a), and (c) continuously adding at least one alkylene oxide and carbon dioxide to the mixture obtained in the step (b). Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or under a pure carbon dioxide atmosphere, at 90-150[deg] C, (b) adding alkylene oxide to the mixture obtained in the step (a) under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or a pure carbon dioxide atmosphere, at 100-150[deg] C, and (c) continuously adding at least one alkylene oxide and carbon dioxide to the mixture obtained in the step (b). An independent claim is also included for activating DMC catalyst, comprising (i) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under inert gas, atmosphere of inert gas-carbon dioxide mixture, or pure carbon dioxide atmosphere, and subsequently (ii) adding alkylene oxide to the mixture obtained in the step (i) under an inert gas, an atmosphere of inert gas-carbon dioxide mixture, or a pure carbon dioxide atmosphere at 90-150[deg] C.
Die vorliegende Erfindung betrifft ein Verfahren zur Aktivierung von Doppelmetallcyanid (DMC)-Katalysatoren mit Heterokumulenen für die Herstellung von Polyethercarbonatpolyolen durch katalytische Copolymerisation von Kohlendioxid (CO 2 ) mit Alkylenoxiden in Gegenwart einer oder mehrerer H-funktioneller Startersubstanzen, sowie ein Verfahren zur Herstellung von Polyethercarbonatpolyolen aus einer oder mehreren H-funktionellen Startersubstanzen, eines oder mehrerer Alkylenoxiden und Kohlendioxid in Gegenwart eines Doppelmetallcyanid-Katalysators, dadurch gekennzeichnet, dass
(±) unter Inertgasatmosphäre, unter einer Atmosphäre aus Inertgas-Kohlendioxid-Gemisch oder unter einer reinen Kohlendioxid-Atmosphäre bei Temperaturen von 90 bis 150°C der DMC-Katalysator mit Heterokumulen und H-funktioneller Startersubstanz vermischt wird,
(²) zu dem Gemisch aus Schritt (±) unter Inertgasatmosphäre, unter einer Atmosphäre aus Inertgas-Kohlendioxid-Gemisch oder unter einer reinen Kohlendioxid-Atmosphäre Alkylenoxid bei Temperaturen von 100 bis 150°C zugegeben wird, und
(³) ein oder mehrere Alkylenoxide und Kohlendioxid zu der aus Schritt (²) resultierenden Mischung fortwährend dosiert werden.</description><subject>CHEMISTRY</subject><subject>COMPOSITIONS BASED THEREON</subject><subject>MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS</subject><subject>METALLURGY</subject><subject>ORGANIC MACROMOLECULAR COMPOUNDS</subject><subject>THEIR PREPARATION OR CHEMICAL WORKING-UP</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>2013</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZAj0TS3JyE9RSMsvUkhMLsksSyzJzEtXSMkvTcpJVchNLUnMUUiuTMzLTElVSE4E8iqLS4oVSvIVCoryU0qTUxUK8nMqgUakFoFZ-TnFPAysaYk5xam8UJqbQcHNNcTZQze1ID8-tbggMTk1L7Uk3jXAyNTEwtLA1NHQmAglAKwaN_o</recordid><startdate>20130123</startdate><enddate>20130123</enddate><creator>LEITNER, WALTER DR</creator><creator>BARRUET, JULIEN DR</creator><creator>MUELLER, THOMAS, ERNST DR</creator><creator>GUERTLER, CHRISTOPH DR</creator><creator>KOEHLER, BURKHARD DR</creator><creator>DIENES, YVONNE DR</creator><scope>EVB</scope></search><sort><creationdate>20130123</creationdate><title>Method for activating double metal cyanide catalysts to produce polyether polyols</title><author>LEITNER, WALTER DR ; BARRUET, JULIEN DR ; MUELLER, THOMAS, ERNST DR ; GUERTLER, CHRISTOPH DR ; KOEHLER, BURKHARD DR ; DIENES, YVONNE DR</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_EP2548905A13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>eng ; fre ; ger</language><creationdate>2013</creationdate><topic>CHEMISTRY</topic><topic>COMPOSITIONS BASED THEREON</topic><topic>MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONSONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS</topic><topic>METALLURGY</topic><topic>ORGANIC MACROMOLECULAR COMPOUNDS</topic><topic>THEIR PREPARATION OR CHEMICAL WORKING-UP</topic><toplevel>online_resources</toplevel><creatorcontrib>LEITNER, WALTER DR</creatorcontrib><creatorcontrib>BARRUET, JULIEN DR</creatorcontrib><creatorcontrib>MUELLER, THOMAS, ERNST DR</creatorcontrib><creatorcontrib>GUERTLER, CHRISTOPH DR</creatorcontrib><creatorcontrib>KOEHLER, BURKHARD DR</creatorcontrib><creatorcontrib>DIENES, YVONNE DR</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>LEITNER, WALTER DR</au><au>BARRUET, JULIEN DR</au><au>MUELLER, THOMAS, ERNST DR</au><au>GUERTLER, CHRISTOPH DR</au><au>KOEHLER, BURKHARD DR</au><au>DIENES, YVONNE DR</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Method for activating double metal cyanide catalysts to produce polyether polyols</title><date>2013-01-23</date><risdate>2013</risdate><abstract>Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or a pure carbon dioxide atmosphere, (b) adding alkylene oxide to the mixture obtained in the step (a), and (c) continuously adding at least one alkylene oxide and carbon dioxide to the mixture obtained in the step (b). Preparing polyether carbonate polyol from at least one hydrogen-functional starter substance, at least one alkylene oxide, and carbon dioxide in presence of double metal cyanide (DMC) catalyst, comprises (a) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or under a pure carbon dioxide atmosphere, at 90-150[deg] C, (b) adding alkylene oxide to the mixture obtained in the step (a) under an inert gas, an atmosphere of inert gas and carbon dioxide mixture, or a pure carbon dioxide atmosphere, at 100-150[deg] C, and (c) continuously adding at least one alkylene oxide and carbon dioxide to the mixture obtained in the step (b). An independent claim is also included for activating DMC catalyst, comprising (i) mixing the DMC catalyst with hetero cumulene and hydrogen-functional starter substance under inert gas, atmosphere of inert gas-carbon dioxide mixture, or pure carbon dioxide atmosphere, and subsequently (ii) adding alkylene oxide to the mixture obtained in the step (i) under an inert gas, an atmosphere of inert gas-carbon dioxide mixture, or a pure carbon dioxide atmosphere at 90-150[deg] C.
Die vorliegende Erfindung betrifft ein Verfahren zur Aktivierung von Doppelmetallcyanid (DMC)-Katalysatoren mit Heterokumulenen für die Herstellung von Polyethercarbonatpolyolen durch katalytische Copolymerisation von Kohlendioxid (CO 2 ) mit Alkylenoxiden in Gegenwart einer oder mehrerer H-funktioneller Startersubstanzen, sowie ein Verfahren zur Herstellung von Polyethercarbonatpolyolen aus einer oder mehreren H-funktionellen Startersubstanzen, eines oder mehrerer Alkylenoxiden und Kohlendioxid in Gegenwart eines Doppelmetallcyanid-Katalysators, dadurch gekennzeichnet, dass
(±) unter Inertgasatmosphäre, unter einer Atmosphäre aus Inertgas-Kohlendioxid-Gemisch oder unter einer reinen Kohlendioxid-Atmosphäre bei Temperaturen von 90 bis 150°C der DMC-Katalysator mit Heterokumulen und H-funktioneller Startersubstanz vermischt wird,
(²) zu dem Gemisch aus Schritt (±) unter Inertgasatmosphäre, unter einer Atmosphäre aus Inertgas-Kohlendioxid-Gemisch oder unter einer reinen Kohlendioxid-Atmosphäre Alkylenoxid bei Temperaturen von 100 bis 150°C zugegeben wird, und
(³) ein oder mehrere Alkylenoxide und Kohlendioxid zu der aus Schritt (²) resultierenden Mischung fortwährend dosiert werden.</abstract><oa>free_for_read</oa></addata></record> |
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title | Method for activating double metal cyanide catalysts to produce polyether polyols |
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