PROCESS FOR PREPARING THE TRIS(DIBENZYLIDENEACETONE)DIPALLADIUM CHLOROFORM COMPLEX

The present invention provides a process for the preparation of Pd2(dba)3.CHCl3 comprising the steps of: (a) reacting a Pd(II) complex with an alkali metal halide in at least one alcohol solvent; and (b) reacting the product of step (a) with a mixture comprising dibenzylideneacetone, chloroform and...

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Bibliographische Detailangaben
1. Verfasser: COLACOT, THOMAS, JOHN
Format: Patent
Sprache:eng ; fre ; ger
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Zusammenfassung:The present invention provides a process for the preparation of Pd2(dba)3.CHCl3 comprising the steps of: (a) reacting a Pd(II) complex with an alkali metal halide in at least one alcohol solvent; and (b) reacting the product of step (a) with a mixture comprising dibenzylideneacetone, chloroform and an inorganic base to form Pd2(dba)3.CHCl3.