PROCESS FOR THE SEPARATION BY DISTILLATION OF DINITROTOLUENE FROM PROCESS WASTEWATER FROM THE PREPARATION OF DINITROTOLUENE BY NITRATION OF TOLUENE BY MEANS OF NITRATING ACID

PROCESS FOR THE SEPARATION BY DISTILLATION OF DINITROTOLUENE FROM PROCESS WASTEWATER FROM THE PREPARATION OF DINITROTOLUENE BY NITRATION OF TOLUENE BY MEANS OF NITRATING ACID

A process is proposed for distillatively removing dinitrotoluene from process wastewater from the preparation of dinitrotoluene by nitrating toluene with nitrating acid, which comprises basifying the process wastewater to a pH of >8.5, feeding it to a stripping column in the upper region thereof...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: PENZEL, ULRICH, ADAM, JOHANNES, FRITZ, RUEDIGER, MERTEN, ANNE-KATHRIN, ALLARDT, HOLGER
Format: Patent
Sprache:eng ; fre ; ger
Schlagworte:
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
PERFORMING OPERATIONS
PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
SEPARATION
TRANSPORTING
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Beschreibung
Zusammenfassung:A process is proposed for distillatively removing dinitrotoluene from process wastewater from the preparation of dinitrotoluene by nitrating toluene with nitrating acid, which comprises basifying the process wastewater to a pH of >8.5, feeding it to a stripping column in the upper region thereof and stripping it with steam in countercurrent to obtain a vapor stream laden with dinitrotoluene and a bottom stream depleted in dinitrotoluene compared to the process wastewater used.