Method of controlling final grain size in supersolvus heat treated nickel-base superalloys and articles formed thereby

A method of forming a component from a gamma-prime precipitation-strengthened nickel-base superalloy so that, following a supersolvus heat treatment, the component characterized by a uniformly-sized grain microstructure. The method includes forming a billet having a sufficiently fine grain size to a...

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Hauptverfasser: HURON, ERIC SCOTT, BAIN, KENNETH REES, MOURER, DAVID PAUL, GROH, JON RAYMOND, SRIVATSA, SHESH KRISHNA, MICKLE, BRIAN FRANCIS
Format: Patent
Sprache:eng ; fre ; ger
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Zusammenfassung:A method of forming a component from a gamma-prime precipitation-strengthened nickel-base superalloy so that, following a supersolvus heat treatment, the component characterized by a uniformly-sized grain microstructure. The method includes forming a billet having a sufficiently fine grain size to achieve superplasticity of the superalloy during a subsequent working step. The billet is then worked at a temperature below the gamma-prime solvus temperature of the superalloy so as to form a worked article, wherein the billet is worked so as to maintain strain rates above a lower strain rate limit to control average grain size and below an upper strain rate limit to avoid critical grain growth. Thereafter, the worked article is heat treated at a temperature above the gamma-prime solvus temperature of the superalloy for a duration sufficient to uniformly coarsen the grains of the worked article, after which the worked article is cooled at a rate sufficient to reprecipitate gamma-prime within the worked article.