PROCESS FOR PREPARING FLUOROCHEMICAL MONOISOCYANATES

A process for preparing fluorochemical monoisocyanates comprises reacting at least one fluorochemical alcohol represented by the formula CnF2n+1SO2NCH3(CH2)mOH, wherein n=2 to 5, and m=2 to 4, with 4,4'-diphenylmethane diisocyanate (MDI) in a solvent in which the resulting fluorochemical monois...

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Bibliographische Detailangaben
Hauptverfasser: KIRK, ALAN, R, KLUN, THOMAS, P, MOORE, GEORGE G., I, CLARK, JOHN, C, QIU, ZAI-MING
Format: Patent
Sprache:eng ; fre ; ger
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Zusammenfassung:A process for preparing fluorochemical monoisocyanates comprises reacting at least one fluorochemical alcohol represented by the formula CnF2n+1SO2NCH3(CH2)mOH, wherein n=2 to 5, and m=2 to 4, with 4,4'-diphenylmethane diisocyanate (MDI) in a solvent in which the resulting fluorochemical monoisocyanate is not soluble; wherein the molar ratio of fluorochemical alcohol:MDI is from about 1:1 to about 1:2.5.