Method of elution of fluorinated emulgators

Elution of fluorinated emulsifiers from anionic exchange resins is effected using a mixture comprising: (a) water; (b) an alkali metal or alkylammonium compound; and (c) an organic solvent which completely dissolves (a) and (b). Elution of fluorinated emulsifiers from anionic exchange resins is effe...

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Bibliographische Detailangaben
Hauptverfasser: LOEHR, GERNOT, SCHWERTFEGER, WERNER, FUEHRER, STEPHAN
Format: Patent
Sprache:eng ; fre ; ger
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Zusammenfassung:Elution of fluorinated emulsifiers from anionic exchange resins is effected using a mixture comprising: (a) water; (b) an alkali metal or alkylammonium compound; and (c) an organic solvent which completely dissolves (a) and (b). Elution of fluorinated emulsifiers from anionic exchange resins is effected using a mixture comprising: (a) water; (b) a compound MX; and (c) an organic solvent which completely dissolves (a) and (b) and gives sufficient anions X for the elution. M = an alkali metal or alkylammonium with 1-4C alkyl; X = OH, F or Cl; An Independent claim is also included for processing the eluate by: (i) steam distilling to remove the volatiles; and (ii) treating the distillation residue with strong acid to set the emulsifiers free in free acid form.