LATE ADDITION OF SUPPLEMENTAL ETHYLENE GLYCOL IN THE PREPARATION OF COPOLYESTERS

The invention is directed to a method for making copolyesters of terephthalic acid and a diol component including ethylene glycol and includes the steps of adding terephthalic acid and diol to a first esterification reactor and then late addition of supplemental ethylene glycol subsequent to the fir...

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Bibliographische Detailangaben
Hauptverfasser: GREENE, CAROL, JULLIARD, JERNIGAN, MARY, THERESE, WINDES, LARRY, CATES
Format: Patent
Sprache:eng ; fre ; ger
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Beschreibung
Zusammenfassung:The invention is directed to a method for making copolyesters of terephthalic acid and a diol component including ethylene glycol and includes the steps of adding terephthalic acid and diol to a first esterification reactor and then late addition of supplemental ethylene glycol subsequent to the first esterification reactor but prior to a point where the ethylene glycol partial pressure is reduced below about 300 torr.