LATE ADDITION OF SUPPLEMENTAL ETHYLENE GLYCOL IN THE PREPARATION OF COPOLYESTERS
The invention is directed to a method for making copolyesters of terephthalic acid and a diol component including ethylene glycol and includes the steps of adding terephthalic acid and diol to a first esterification reactor and then late addition of supplemental ethylene glycol subsequent to the fir...
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Format: | Patent |
Sprache: | eng ; fre ; ger |
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Zusammenfassung: | The invention is directed to a method for making copolyesters of terephthalic acid and a diol component including ethylene glycol and includes the steps of adding terephthalic acid and diol to a first esterification reactor and then late addition of supplemental ethylene glycol subsequent to the first esterification reactor but prior to a point where the ethylene glycol partial pressure is reduced below about 300 torr. |
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