Process for the preparation of high purity 1,3-dialkyl-2-imidazolidinone

In a process for reacting N,N'-dialkylethylenediamine with urea in an aprotic polar solvent to prepare 1,3-dialkyl-2-imidazolidinone, a process comprising progressing the reaction while continuously adding N,N'-dialkylethylenediamine and urea into the aprotic polar solvent, is disclosed. T...

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Hauptverfasser: MIZUTA, HIDEKI, TAKAOKA, MASAZUMI, NAGATA, TERUYUKI
Format: Patent
Sprache:eng ; fre ; ger
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Zusammenfassung:In a process for reacting N,N'-dialkylethylenediamine with urea in an aprotic polar solvent to prepare 1,3-dialkyl-2-imidazolidinone, a process comprising progressing the reaction while continuously adding N,N'-dialkylethylenediamine and urea into the aprotic polar solvent, is disclosed. The process is a high-yield manufacturing process in industry capable of efficiently producing very high purity 1,3-dialkyl-2-imidazolidinone which contains less than 0.1% by weight of by-product 1,3-dialkyl-2-imidazolidinimine derived from the raw materials.