Process for the purification of 1,1-dichloro-1-fluoroethane

Purificn. of CCl2FCH3 comprises: (a) reacting anhydrous HF with CCl3CH3 or vinylidene chloride contg. dichloroacetylene to form CCl2FCH3; and (b) passing the CCl2FCH3 through activated C to remove unsatd. impurities. The unsatd. impurities are pred. dichloroacetylene and/or vinylidene chloride. The...

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Bibliographische Detailangaben
Hauptverfasser: SMITH, ADDISON MILES, TUNG, HSUEH SUNG
Format: Patent
Sprache:eng ; fre ; ger
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Zusammenfassung:Purificn. of CCl2FCH3 comprises: (a) reacting anhydrous HF with CCl3CH3 or vinylidene chloride contg. dichloroacetylene to form CCl2FCH3; and (b) passing the CCl2FCH3 through activated C to remove unsatd. impurities. The unsatd. impurities are pred. dichloroacetylene and/or vinylidene chloride. The activated C pref. has particle size range of 0.005-10 mm, most pref. 0.1-2 mm.