PROCESS FOR SILVER CATHODE ACTIVATION

Silver cathodes used in electrochemical synthesis are activated or reactivated after a period of use by immersion in a dilute alkaline aqueous solution of a compatible oxidizing agent. An expanded silver sheet cathode in an electrolytic cell used for the conversion of 3,4,5,6-tetrachloropicolinic ac...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: BON, CHARLES K, KNOWLES, VERA M
Format: Patent
Sprache:eng
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:Silver cathodes used in electrochemical synthesis are activated or reactivated after a period of use by immersion in a dilute alkaline aqueous solution of a compatible oxidizing agent. An expanded silver sheet cathode in an electrolytic cell used for the conversion of 3,4,5,6-tetrachloropicolinic acid to the herbicide 3,6-dichloropicolinic acid was reactivated by circulating an aqueous solution containing about 0.5 percent sodium hypochlorite and about 2 percent sodium hydroxide through the cell.