PROCESS FOR SILVER CATHODE ACTIVATION
Silver cathodes used in electrochemical synthesis are activated or reactivated after a period of use by immersion in a dilute alkaline aqueous solution of a compatible oxidizing agent. An expanded silver sheet cathode in an electrolytic cell used for the conversion of 3,4,5,6-tetrachloropicolinic ac...
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Zusammenfassung: | Silver cathodes used in electrochemical synthesis are activated or reactivated after a period of use by immersion in a dilute alkaline aqueous solution of a compatible oxidizing agent. An expanded silver sheet cathode in an electrolytic cell used for the conversion of 3,4,5,6-tetrachloropicolinic acid to the herbicide 3,6-dichloropicolinic acid was reactivated by circulating an aqueous solution containing about 0.5 percent sodium hypochlorite and about 2 percent sodium hydroxide through the cell. |
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