Process for recovery of acetone

This invention is a process for purifying crude acetone obtained by cleavage of cumene hydroperoxide, said crude acetone containing aldehyde impurities and appreciable amounts of unreacted cumene, by fractionally distilling the acetone in a multiple plate distillation column, said process comprising...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser: HINTON, EVERETT HAWTHORNE JR, CHAN, CHONG HUI, CRESCENTINI, LAMBERTO
Format: Patent
Sprache:eng ; fre ; ger
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Beschreibung
Zusammenfassung:This invention is a process for purifying crude acetone obtained by cleavage of cumene hydroperoxide, said crude acetone containing aldehyde impurities and appreciable amounts of unreacted cumene, by fractionally distilling the acetone in a multiple plate distillation column, said process comprising: continuously feeding crude acetone; continuously feeding a dilute aqueous solution of an alkaline material at a point above the crude acetone feed point; and controlling the temperature profile of the column by adjusting the amount of liquid acetone removed in step (c) to maintain a preselected temperature on a plate in the region between the crude acetone feed point and the alkaline material feed point.