METHOD FOR DETERMINING THE CONTENT OF HYDROGEN DISULFIDE IN CRUDE AND RESIDUAL OILS

The subject of the invention is a method for determining the HS content arising during the warm storage of sulfur-containing crude and residual oils and mineral distillates containing sulfur-containing crude and/or residual oils, in which a sample of the sulfur-containing mineral oil is dissolved in...

Ausführliche Beschreibung

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Bibliographische Detailangaben
Hauptverfasser:	KRULL MATTHIAS, FEUSTEL MICHAEL, BRAUCHLE MICHAEL, ANDRIN DOMINKO
Format:	Patent
Sprache:	eng ; rus
Schlagworte:	CHEMISTRY CRACKING HYDROCARBON OILS FUELS GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIRCHEMICAL OR PHYSICAL PROPERTIES LUBRICANTS MEASURING METALLURGY MINERAL WAXES PEAT PERFORMING OPERATIONS PETROLEUM, GAS OR COKE INDUSTRIES PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL PHYSICS PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVEHYDROGENATION, OLIGOMERISATION, POLYMERISATION RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, ORGASES REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS REFORMING OF NAPHTHA SEPARATION TECHNICAL GASES CONTAINING CARBON MONOXIDE TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION TECHNICAL SUBJECTS COVERED BY FORMER USPC TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS TESTING TRANSPORTING
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Beschreibung
Zusammenfassung:	The subject of the invention is a method for determining the HS content arising during the warm storage of sulfur-containing crude and residual oils and mineral distillates containing sulfur-containing crude and/or residual oils, in which a sample of the sulfur-containing mineral oil is dissolved in a solvent or solvent mixture that boils at more than 200°C and a carrier gas is caused to flow through the solution of the sulfur-containing mineral oil at temperatures above 80°C, and the quantity of hydrogen disulfide carried out with the carrier gas is analyzed quantitatively. Целью изобретения является способ определения содержания HS, образующегося при хранении в тёплом складе серосодержащих сырой нефти и кубовым остатком и нефтяных дистиллятов, содержащих серосодержащие сырую нефть и/или кубовые остатки, в котором образец серосодержащего нефтепродукта растворяют в растворителе или смеси растворителей, которые кипят выше 200°С, и газ-носитель должен проходить через раствор серосодержащего нефтепродукта при температуре выше 80°С, и количество сероводорода, выделенного газом-носителем, количественно определяют.