Verfahren zur Herstellung eines Cyclohexanonoxim/Cyclododecanonoxim-Gemisches

Verfahren zur Herstellung eines Cyclohexanonoxim/Cyclododecanonoxim-Gemisches

Process for preparing a mixture of cyclohexanoneoxime-cyclododecanoneoxime containing at the most 70 parts by weight of cyclododecanoneoxime, by oximation of cyclohexanone and cyclododecanone with hydroxylamine sulfate, which comprises carrying out the oximation in two stages, the first stage being...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Hauptverfasser: HUERLIMANN,ERNST,DR.SC.TECHN, SCHULTZE,HANS-JOACHIM,.ER.NAT, GEHRING,ALBERT,-MASCH
Format: Patent
Sprache:ger
Schlagworte:
ACYCLIC OR CARBOCYCLIC COMPOUNDS
CHEMISTRY
METALLURGY
ORGANIC CHEMISTRY
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:Process for preparing a mixture of cyclohexanoneoxime-cyclododecanoneoxime containing at the most 70 parts by weight of cyclododecanoneoxime, by oximation of cyclohexanone and cyclododecanone with hydroxylamine sulfate, which comprises carrying out the oximation in two stages, the first stage being effected at a pH of 3-4.5 and 80 DEG -90 DEG C, and the second stage at a pH of 5-6 and a temperature of 90 DEG -110 DEG C.