Trinitrochlorobenzene from phosphorus- - oxychloride pyridine and picric acid

The reagents are reacted at 90-95 degrees C in the following proportions: phosphorus arcyhloride, 3 mole; pyridine 1-1.2 mole; picric acid, 1 mole. The process avoids the use of volatile, inflammable solvents. Product is an explosive.

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Bibliographische Detailangaben
Hauptverfasser: DEISENROTH,ULF, KARL MEYER,DR
Format: Patent
Sprache:eng ; ger
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Zusammenfassung:The reagents are reacted at 90-95 degrees C in the following proportions: phosphorus arcyhloride, 3 mole; pyridine 1-1.2 mole; picric acid, 1 mole. The process avoids the use of volatile, inflammable solvents. Product is an explosive.