Verfahren zur Herstellung von als optische Aufheller verwendbaren Azolverbindungen

The invention comprises compounds of the formula and the production of compounds of the formula where R is a 4,41-stilbene radical, A is an o-phenylene radical and X is 0 or 5, by heating HOOC-R-COOH with HX-A-NH2.(HCl)m (where m is 0 or 1) and a halogenating agent capable of converting COOH to ac...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
1. Verfasser: SIGMUND BLOOM,MELVIN
Format: Patent
Sprache:ger
Schlagworte:
Online-Zugang:Volltext bestellen
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page
container_issue
container_start_page
container_title
container_volume
creator SIGMUND BLOOM,MELVIN
description The invention comprises compounds of the formula and the production of compounds of the formula where R is a 4,41-stilbene radical, A is an o-phenylene radical and X is 0 or 5, by heating HOOC-R-COOH with HX-A-NH2.(HCl)m (where m is 0 or 1) and a halogenating agent capable of converting COOH to acid halide, e.g. POCl3, to form an intermediate condensation product, and then refluxing to form the product. A solvent may be used, e.g. 1,2,4-trichlorobenzene. Both R and/or A may be substituted; many possible substituents are given. In examples, X is 0 or S and R and A are unsubstituted; and X is 0, R is unsubstituted, and A is phenyl-substituted. The products may be mixed with soaps or detergents for increasing fabric brightness or whiteness.
format Patent
fullrecord <record><control><sourceid>epo_EVB</sourceid><recordid>TN_cdi_epo_espacenet_DE1445699A1</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>DE1445699A1</sourcerecordid><originalsourceid>FETCH-epo_espacenet_DE1445699A13</originalsourceid><addsrcrecordid>eNrjZAgKSy1KS8woSs1TqCotUvBILSouSc3JKc1LVyjLz1NIzClWyC8oySxOzkhVcCxNywDKpRYplKUWlafmpSQlgvQ5VuXnAAWSMvNSgNpS83gYWNOA-lJ5oTQ3g4Kba4izh25qQX58anFBYnJqXmpJvIuroYmJqZmlpaOhMRFKAA9qOI4</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>patent</recordtype></control><display><type>patent</type><title>Verfahren zur Herstellung von als optische Aufheller verwendbaren Azolverbindungen</title><source>esp@cenet</source><creator>SIGMUND BLOOM,MELVIN</creator><creatorcontrib>SIGMUND BLOOM,MELVIN</creatorcontrib><description>The invention comprises compounds of the formula &lt;FORM:1072919/C2/1&gt; and the production of compounds of the formula &lt;FORM:1072919/C2/2&gt; where R is a 4,41-stilbene radical, A is an o-phenylene radical and X is 0 or 5, by heating HOOC-R-COOH with HX-A-NH2.(HCl)m (where m is 0 or 1) and a halogenating agent capable of converting COOH to acid halide, e.g. POCl3, to form an intermediate condensation product, and then refluxing to form the product. A solvent may be used, e.g. 1,2,4-trichlorobenzene. Both R and/or A may be substituted; many possible substituents are given. In examples, X is 0 or S and R and A are unsubstituted; and X is 0, R is unsubstituted, and A is phenyl-substituted. The products may be mixed with soaps or detergents for increasing fabric brightness or whiteness.</description><language>ger</language><subject>BLEACHING LEATHER OR FURS ; CHEMISTRY ; DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS,YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS ; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR ; HETEROCYCLIC COMPOUNDS ; LAUNDERING ; METALLURGY ; ORGANIC CHEMISTRY ; TEXTILES ; TREATMENT OF TEXTILES OR THE LIKE</subject><creationdate>1968</creationdate><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=19681205&amp;DB=EPODOC&amp;CC=DE&amp;NR=1445699A1$$EHTML$$P50$$Gepo$$Hfree_for_read</linktohtml><link.rule.ids>230,308,776,881,25543,76293</link.rule.ids><linktorsrc>$$Uhttps://worldwide.espacenet.com/publicationDetails/biblio?FT=D&amp;date=19681205&amp;DB=EPODOC&amp;CC=DE&amp;NR=1445699A1$$EView_record_in_European_Patent_Office$$FView_record_in_$$GEuropean_Patent_Office$$Hfree_for_read</linktorsrc></links><search><creatorcontrib>SIGMUND BLOOM,MELVIN</creatorcontrib><title>Verfahren zur Herstellung von als optische Aufheller verwendbaren Azolverbindungen</title><description>The invention comprises compounds of the formula &lt;FORM:1072919/C2/1&gt; and the production of compounds of the formula &lt;FORM:1072919/C2/2&gt; where R is a 4,41-stilbene radical, A is an o-phenylene radical and X is 0 or 5, by heating HOOC-R-COOH with HX-A-NH2.(HCl)m (where m is 0 or 1) and a halogenating agent capable of converting COOH to acid halide, e.g. POCl3, to form an intermediate condensation product, and then refluxing to form the product. A solvent may be used, e.g. 1,2,4-trichlorobenzene. Both R and/or A may be substituted; many possible substituents are given. In examples, X is 0 or S and R and A are unsubstituted; and X is 0, R is unsubstituted, and A is phenyl-substituted. The products may be mixed with soaps or detergents for increasing fabric brightness or whiteness.</description><subject>BLEACHING LEATHER OR FURS</subject><subject>CHEMISTRY</subject><subject>DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS,YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS</subject><subject>FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR</subject><subject>HETEROCYCLIC COMPOUNDS</subject><subject>LAUNDERING</subject><subject>METALLURGY</subject><subject>ORGANIC CHEMISTRY</subject><subject>TEXTILES</subject><subject>TREATMENT OF TEXTILES OR THE LIKE</subject><fulltext>true</fulltext><rsrctype>patent</rsrctype><creationdate>1968</creationdate><recordtype>patent</recordtype><sourceid>EVB</sourceid><recordid>eNrjZAgKSy1KS8woSs1TqCotUvBILSouSc3JKc1LVyjLz1NIzClWyC8oySxOzkhVcCxNywDKpRYplKUWlafmpSQlgvQ5VuXnAAWSMvNSgNpS83gYWNOA-lJ5oTQ3g4Kba4izh25qQX58anFBYnJqXmpJvIuroYmJqZmlpaOhMRFKAA9qOI4</recordid><startdate>19681205</startdate><enddate>19681205</enddate><creator>SIGMUND BLOOM,MELVIN</creator><scope>EVB</scope></search><sort><creationdate>19681205</creationdate><title>Verfahren zur Herstellung von als optische Aufheller verwendbaren Azolverbindungen</title><author>SIGMUND BLOOM,MELVIN</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-epo_espacenet_DE1445699A13</frbrgroupid><rsrctype>patents</rsrctype><prefilter>patents</prefilter><language>ger</language><creationdate>1968</creationdate><topic>BLEACHING LEATHER OR FURS</topic><topic>CHEMISTRY</topic><topic>DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS,YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS</topic><topic>FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR</topic><topic>HETEROCYCLIC COMPOUNDS</topic><topic>LAUNDERING</topic><topic>METALLURGY</topic><topic>ORGANIC CHEMISTRY</topic><topic>TEXTILES</topic><topic>TREATMENT OF TEXTILES OR THE LIKE</topic><toplevel>online_resources</toplevel><creatorcontrib>SIGMUND BLOOM,MELVIN</creatorcontrib><collection>esp@cenet</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>SIGMUND BLOOM,MELVIN</au><format>patent</format><genre>patent</genre><ristype>GEN</ristype><title>Verfahren zur Herstellung von als optische Aufheller verwendbaren Azolverbindungen</title><date>1968-12-05</date><risdate>1968</risdate><abstract>The invention comprises compounds of the formula &lt;FORM:1072919/C2/1&gt; and the production of compounds of the formula &lt;FORM:1072919/C2/2&gt; where R is a 4,41-stilbene radical, A is an o-phenylene radical and X is 0 or 5, by heating HOOC-R-COOH with HX-A-NH2.(HCl)m (where m is 0 or 1) and a halogenating agent capable of converting COOH to acid halide, e.g. POCl3, to form an intermediate condensation product, and then refluxing to form the product. A solvent may be used, e.g. 1,2,4-trichlorobenzene. Both R and/or A may be substituted; many possible substituents are given. In examples, X is 0 or S and R and A are unsubstituted; and X is 0, R is unsubstituted, and A is phenyl-substituted. The products may be mixed with soaps or detergents for increasing fabric brightness or whiteness.</abstract><oa>free_for_read</oa></addata></record>
fulltext fulltext_linktorsrc
identifier
ispartof
issn
language ger
recordid cdi_epo_espacenet_DE1445699A1
source esp@cenet
subjects BLEACHING LEATHER OR FURS
CHEMISTRY
DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS,YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS
FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
HETEROCYCLIC COMPOUNDS
LAUNDERING
METALLURGY
ORGANIC CHEMISTRY
TEXTILES
TREATMENT OF TEXTILES OR THE LIKE
title Verfahren zur Herstellung von als optische Aufheller verwendbaren Azolverbindungen
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-24T04%3A29%3A22IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-epo_EVB&rft_val_fmt=info:ofi/fmt:kev:mtx:patent&rft.genre=patent&rft.au=SIGMUND%20BLOOM,MELVIN&rft.date=1968-12-05&rft_id=info:doi/&rft_dat=%3Cepo_EVB%3EDE1445699A1%3C/epo_EVB%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true