Method for producing hydroxylammonium salts

A method of producing hydroxylammonium salts by catalytic reaction of nitrogen monoxide with hydrogen in a diluted aqueous solution of mineral acid in the presence of platinum catalysts suspended on a support in multiple subsequent reaction stages. This reaction takes place in a stirred reactor wher...

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Bibliographische Detailangaben
1. Verfasser: LOEBEL WOLFGANG,STRECKER THOMAS,SEIDLER JOACHIM
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:A method of producing hydroxylammonium salts by catalytic reaction of nitrogen monoxide with hydrogen in a diluted aqueous solution of mineral acid in the presence of platinum catalysts suspended on a support in multiple subsequent reaction stages. This reaction takes place in a stirred reactor wherein a gas inlet and distribution system is provided in the lower part of the stirred reactor, a disk agitator is placed immediately above, the hub with bearing surface or support mounting angled, concave and tilted agitator blades that rotate their angled or concave sides in the direction of motion, and a two-blade agitator is provided on the agitator shaft in the upper part of the stirred reactor, its individual leaves being offset like lamellas so that they constantly wet the reactor cap when rotating.