Method for separating an esterification catalyst

A method for removing esterification catalyst from crude plasticizer ester based on dicarboxylic acid and 8-13C alcohols, by treatment with aqueous alkali at 10-100 degrees C followed by separation of the hydrolyzed catalyst-containing aqueous phase under gravity, in which the crude ester is treated...

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Bibliographische Detailangaben
Hauptverfasser: GOLFIER GUENTHER, PETERS JARREN, SCHWIRTEN KURT, DISTELDORF WALTER
Format: Patent
Sprache:eng
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Beschreibung
Zusammenfassung:A method for removing esterification catalyst from crude plasticizer ester based on dicarboxylic acid and 8-13C alcohols, by treatment with aqueous alkali at 10-100 degrees C followed by separation of the hydrolyzed catalyst-containing aqueous phase under gravity, in which the crude ester is treated before or during phase separation with salts(s) of di- or multi-valent metal(s).