Method for synthesizing nickel tetracarbonyl
The invention relates to a compound method for nickel carbonoxide. It sets thermalloy or ambrose first alloy onto fixed bed reactor and is continuously pumped into carbon monoxide with catalyst. The reaction pressure is controlled from 5.0Mpa to 15.0Mpa, and temperature is controlled from 150 degree...
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Sprache: | eng |
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Zusammenfassung: | The invention relates to a compound method for nickel carbonoxide. It sets thermalloy or ambrose first alloy onto fixed bed reactor and is continuously pumped into carbon monoxide with catalyst. The reaction pressure is controlled from 5.0Mpa to 15.0Mpa, and temperature is controlled from 150 degree centigrade to 250 degree centigrade. Thus, the carbonylation ratio of nickel in raw material is very high. And experiment safety factor is sharply increased. |
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