Method for preparing superfine nickel carbonyl powder by nickel carbonyl thermal decomposition

The invention discloses a method that is used to prepare superfine carbonyl nickel powder by the carbonyl nickel thermal decomposition. The method is that the carbonyl nickel and the carbon monoxide gas are mixed admission the decomposer to mix with the carbon monoxide main heat source gas whose preheating temperature is from two hundred and forty centigrade degree to three hundred twenty centigrade degree to make the carbonyl nickel decompose to from superfine carbonyl nickel powder whose granularity is from twenty nanometer to ten millimeter. The pressure of the decomposer is from 0.02MPa to 0.2MPa in the whole decomposition process. The invention avoids the complicated operation of separating the mixed gas after the decomposition, simplifies the preparation technology, reduces the cost of the production, and greatly reduces the produce of the wall built up.